Crystal Structure of 3-Acetoxy-2-methyl-N-(4-nitrophenyl)benzamide

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Kansiz S., ÇAKMAK Ş., DEGE N., Meral G., Kütük H.

X-RAY STRUCTURE ANALYSIS ONLINE, cilt.34, ss.17-18, 2018 (ESCI) identifier identifier

  • Yayın Türü: Makale / Tam Makale
  • Cilt numarası: 34
  • Basım Tarihi: 2018
  • Doi Numarası: 10.2116/xraystruct.34.17
  • Dergi Adı: X-RAY STRUCTURE ANALYSIS ONLINE
  • Derginin Tarandığı İndeksler: Emerging Sources Citation Index (ESCI), Scopus
  • Sayfa Sayıları: ss.17-18
  • Ondokuz Mayıs Üniversitesi Adresli: Evet

Özet

The structure of 3-acetoxy-2-methyl-N-(4-nitrophenyl)benzamide was determined by X-ray crystallography. The compound crystallized in a monoclinic system and it was characterized in the space group P2(1)/c with cell parameters a = 5.8658(3), b = 17.1661(10), c = 15.1938(7) angstrom, beta = 103.182(4)degrees, Z = 4, V = 1489.60(14) angstrom(3). The R1 [I > 2 sigma(I)] and wR2 (all data) values are 0.046 and 0.093, respectively, for all 2932 independent reflections. Intramolecular C3-H3 center dot center dot center dot O3 and intermolecular N2-H2 center dot center dot center dot O1, C5-H5 center dot center dot center dot O1 interactions were observed in the crystal lattice.