Structure analysis of O,O'-propane-1,3-diyl bis[diphenyl(phosphinothioate)]

Karaman M., Irisli S., Buyukgungor O.

CRYSTALLOGRAPHY REPORTS, vol.58, no.7, pp.1088-1090, 2013 (SCI-Expanded) identifier identifier

  • Publication Type: Article / Article
  • Volume: 58 Issue: 7
  • Publication Date: 2013
  • Doi Number: 10.1134/s1063774513080051
  • Journal Name: CRYSTALLOGRAPHY REPORTS
  • Journal Indexes: Science Citation Index Expanded (SCI-EXPANDED), Scopus
  • Page Numbers: pp.1088-1090
  • Ondokuz Mayıs University Affiliated: Yes

Abstract

A new diphosphine disulphide compound with the formula C27H26O2|P2S2, was synthesized from the reaction between PPh2SCl and 1,3-propanediol and characterized with different spectroscopic methods. Its structure has also been studied by X-ray diffraction. The compound crystallizes in the triclinic space group . Pentavalent phosphorus atoms in the molecule are in distorted tetrahedral environments.