Synthesis, characterization and thermal behaviour of novel phthalocyanines bearing chalcone groups on peripheral positions
BULGARIAN CHEMICAL COMMUNICATIONS, cilt.47, sa.3, ss.844-848, 2015 (SCI-Expanded, Scopus)
- Yayın Türü: Makale / Tam Makale
- Cilt numarası: 47 Sayı: 3
- Basım Tarihi: 2015
- Dergi Adı: BULGARIAN CHEMICAL COMMUNICATIONS
- Derginin Tarandığı İndeksler: Science Citation Index Expanded (SCI-EXPANDED), Scopus
- Sayfa Sayıları: ss.844-848
- Ondokuz Mayıs Üniversitesi Adresli: Hayır
Özet
A new nickel, zinc, cobalt, copper and metal-free phthalocyanine was synthesized by nucleophilic aromatic substitution reaction of (E)-3-(3-hydroxyphenyl)-1-phenylprop-2-en-1-one with 4-nitrophthalonitrile and cyclotetramerisation of (E)-4-(3-(3-oxo-3-phenylprop-1-enyl)phenoxy) phthalonitrile. The new compounds were characterized by a combination of IR, H-1 NMR, C-13 NMR, UV-Vis, elemental analysis and MS spectral data. The thermal stabilities of the phthalocyanine compounds were determined by thermogravimetric analysis.