Structure of 4,4’-butane-(1,4,7-three-p-tolylsulphonyl-1,4,7-three amine) diphthalonitrile

YILDIRIM S., Işik Ş., Ağar E., Şaşmaz S., Fun H., Erdoönmez A.

Spectroscopy Letters, cilt.33, sa.2, ss.245-254, 2000 (SCI-Expanded) identifier

  • Yayın Türü: Makale / Tam Makale
  • Cilt numarası: 33 Sayı: 2
  • Basım Tarihi: 2000
  • Doi Numarası: 10.1080/00387010009350074
  • Dergi Adı: Spectroscopy Letters
  • Derginin Tarandığı İndeksler: Science Citation Index Expanded (SCI-EXPANDED), Scopus
  • Sayfa Sayıları: ss.245-254
  • Anahtar Kelimeler: Crystal Structure, Phthalocyanines
  • Ondokuz Mayıs Üniversitesi Adresli: Evet

Özet

The crystal structure of the title compound, C41H35N7O6S3 was determined as monoclinic by single crystal X-Ray diffraction technique. The molecular structure was identified by IR, 1H-NMR, 13C-NMR and elemental analysis. The crystal parameters of this compound are as follows: monoclinic P 2 1/n, a = 12.694(2)Å, b = 26.204(2)Å, c = 13.005(2)Å, β = 102.95(2)°, V = 4216.02(1) Å3, Z = 4, Dx = 1.289 g/cm3, F(000) = 1704, λ (MoKα) = 0.71070 Å, μ = 0.2 mm-1. The structure was solved by SHELXS-97 and refined by SHELXL-97. R = 0.06 for 3178 observed reflections with I > 2σ (I).