Synthesis, crystal structure and characterization of hexakis[2-methoxy-4-formylphenoxy]cyclotriphosphazene

Tumer, Yasemin; Bati, Hümeyra; Caliskan, Nezihe; Yueksektepe, Cigdem; Bueyuekguengoer, Orhan

doi:10.1002/zaac.200700389

Synthesis, crystal structure and characterization of hexakis[2-methoxy-4-formylphenoxy]cyclotriphosphazene

Tumer Y., Bati H., Caliskan N., Yueksektepe C., Bueyuekguengoer O.

ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE, cilt.634, sa.3, ss.597-599, 2008 (SCI-Expanded, Scopus)

Yayın Türü: Makale / Tam Makale
Cilt numarası: 634 Sayı: 3
Basım Tarihi: 2008
Doi Numarası: 10.1002/zaac.200700389
Dergi Adı: ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE
Derginin Tarandığı İndeksler: Science Citation Index Expanded (SCI-EXPANDED), Scopus
Sayfa Sayıları: ss.597-599
Anahtar Kelimeler: hexachlorocyclotriphosphazene, crystal structure, 4-hydroxy-3-metlioxy-benzaldehyde, thermal analysis, CYCLOTRIPHOSPHAZENES, PHOSPHAZENES, COORDINATION
Ondokuz Mayıs Üniversitesi Adresli: Evet

Özet

The new cyclotriphosphazene derivative N3P3(OC6H3OCH3COH)(6) (1) was synthesized from hexachlorocyclotriphosphazene, N3P3Cl6, and 4-hydroxy-3-methoxybenzaldehyde in acetonitrile in the presence of K2CO3. The structure of 1 was verified by means of elemental analysis, IR, H-1 NMR, C-13 NMR, P-31 NMR spectra, thermal analysis and X-ray diffraction.