CHARACTERIZATION AND COMPARATIVE STUDIES ON CONVENTIONAL AND MICROWAVE SYNTHESIS OF SOME DISULFIDES

Türköz Karakullukçu N., Yakan H., Öztürk S., Kütük H.

PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS, vol.188, no.11, pp.1576-1583, 2013 (SCI-Expanded) identifier identifier

  • Publication Type: Article / Article
  • Volume: 188 Issue: 11
  • Publication Date: 2013
  • Doi Number: 10.1080/10426507.2013.769984
  • Journal Name: PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS
  • Journal Indexes: Science Citation Index Expanded (SCI-EXPANDED), Scopus, Index Chemicus (IC)
  • Page Numbers: pp.1576-1583
  • Keywords: Disulfides, cysteine, 2-mercaptobenzimidazole, 2-mercaptonicotinic acid, microwave heating, ORGANIC-SYNTHESIS, ASSISTED SYNTHESIS, DERIVATIVES, SULFUR, IRRADIATION, CHEMISTRY, CATALYST, OVENS
  • Ondokuz Mayıs University Affiliated: Yes

Abstract

Some disulfide derivatives have been prepared by microwave assisted synthesis methodology from thiophthalimides(sulfenimides) and thiols in a modified microwave oven under reflux at 600 Watt in ethanol. Elucidation of the structures of the synthesized compounds has been performed by IR, H-1 NMR, and C-13 NMR spectroscopic methods. [Supplemental materials are available for this article. Go to the publisher's online edition of Phosphorus, Sulfur, and Silicon and the Related Elements for the following free supplemental files: Additional figures]